Determination of 15 Rare Earth Elements in Agricultural Crop Samples by Inductively Coupled Plasma Mass Spectrometry—Taking Saffron as an Example
摘要
This study presents a method for the determination of 15 rare earth elements (REEs) in agricultural crops using microwave digestion coupled with inductively coupled plasma mass spectrometry (ICP-MS), with saffron as an example. The detection limit of this method ranged from 0.001 to 0.069 µg g−1, the spiked recovery rate ranged from 91.1 to 106.0%, and the relative standard deviation (RSD, n = 6) ranged from 0.44 to 4.97%, meeting the requirements for trace element analysis. This research provides a rapid and accurate method for analyzing REE content in saffron, offering significant support for studying REE levels in agricultural crops.