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Abstract <p>Photochemical cyclization of <i>N</i>-allyl-<i>N</i>-(2-formylphenyl)-4-methylbenzenesulfonamide in DMSO under irradiation with a light-emitting diode at λ 365 nm afforded 29% of 3-(4-methylbenzenesulfonyl)-1,1a,2,3-tetrahydro-7b<i>H</i>-cyclopropa[<i>c</i>]quinolin-7b-ol. The reaction is diastereoselective, and it requires no catalysis.</p>

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Photochemical Cyclization of N-Allyl-N-(2-formylphenyl)-4-methylbenzenesulfonamide

  • 期刊论文

  • 出版模式：

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  • 发表日期：

    2025年12月1日

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  • D. I. Rudik,
  • A. Yu. Smirnov,
  • A. R. Romanenko,
  • A. A. Korlyukov,
  • M. S. Baranov

摘要

Abstract

Photochemical cyclization of N-allyl-N-(2-formylphenyl)-4-methylbenzenesulfonamide in DMSO under irradiation with a light-emitting diode at λ 365 nm afforded 29% of 3-(4-methylbenzenesulfonyl)-1,1a,2,3-tetrahydro-7bH-cyclopropa[c]quinolin-7b-ol. The reaction is diastereoselective, and it requires no catalysis.