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Abstract <p>A novel composite material based on butadiene-nitrile rubber and silicon carbide (<b>BNR-SiC</b>) was synthesized and used for the first time to determine volatile components of lavender flowers by passive sorption, followed by thermal desorption and gas chromatography−mass spectrometry (<b>GC−MS</b>) identification. This material was demonstrated to capture almost the full range of organic compounds, exhibiting similar sorption/desorption efficiency and better thermal stability compared to Tenax TA. The chromatograms of lavender constituents obtained by passive sorption on Tenax TA and BNR-SiC composite are quite similar. Classes of compounds identified on the chromatograms include mono- and sesquiterpenes, their oxygenated derivatives, terpene alcohols, aromatic hydrocarbons, heterocyclic compounds, phenols, glycerides, linalool, linalyl acetate, eucalyptol, caryophyllene, linalool oxides, 1,3-glyceryl diacetate, and fatty acids, totaling 60 compounds. The approach of passive sorption on a BNR-SiC sorbent followed by thermal desorption GC−MS fingerprint analysis can provide a rough estimation of the compositional diversity and proximity of multi-herbal samples containing various groups of volatile terpene compounds.</p>

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Determination of Volatile Compounds from Lavender Flowers Using Passive Sorption on Novel Monolithic Butadiene-Nitrile Rubber and Silicon Carbide Materials by Thermal Desorption Gas Chromatography–Mass Spectrometry

  • 期刊论文

  • 发表日期：

    2025年4月1日

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  • A. V. Pirogov,
  • E. S. Chichkanova,
  • A. S. Popov,
  • V. V. Levkina,
  • T. A. Bolotnik,
  • M. V. Popik,
  • A. A. Stepashkin,
  • E. N. Grunina,
  • O. M. Zolotilova

摘要

Abstract

A novel composite material based on butadiene-nitrile rubber and silicon carbide (BNR-SiC) was synthesized and used for the first time to determine volatile components of lavender flowers by passive sorption, followed by thermal desorption and gas chromatography−mass spectrometry (GC−MS) identification. This material was demonstrated to capture almost the full range of organic compounds, exhibiting similar sorption/desorption efficiency and better thermal stability compared to Tenax TA. The chromatograms of lavender constituents obtained by passive sorption on Tenax TA and BNR-SiC composite are quite similar. Classes of compounds identified on the chromatograms include mono- and sesquiterpenes, their oxygenated derivatives, terpene alcohols, aromatic hydrocarbons, heterocyclic compounds, phenols, glycerides, linalool, linalyl acetate, eucalyptol, caryophyllene, linalool oxides, 1,3-glyceryl diacetate, and fatty acids, totaling 60 compounds. The approach of passive sorption on a BNR-SiC sorbent followed by thermal desorption GC−MS fingerprint analysis can provide a rough estimation of the compositional diversity and proximity of multi-herbal samples containing various groups of volatile terpene compounds.