Production process of Tiliacora triandra (Diels) flakes via vacuum-assisted freeze-drying technique
摘要
This study evaluates the vacuum-assisted freeze-drying (VFD) process for producing Tiliacora triandra flakes, focusing on the impact of freezing temperatures (–10, − 20, − 30, and − 40 °C) on energy efficiency and product quality. Among the tested conditions, − 20 °C offered the best balance between energy consumption and nutrient retention. During freezing, the sample temperature dropped from 10.4 °C to − 10.9 °C within 240 min, followed by primary drying under vacuum (< 1 mbar) for 600 min, reaching − 21.5 °C with the lowest temperature change rate (0.089 °C/min). Final product temperature stabilized at 27.7 °C during secondary drying. Energy usage increased with decreasing temperature, ranging from 19.9 kWh at − 10 °C to 23 kWh at − 40 °C. At − 20 °C, consumption was 21.5 kWh, equivalent to 90.73 THB per batch. Statistical analysis showed no significant differences in color parameters (p > 0.05), but flakes dried at − 20 °C demonstrated the best color stability (L* = 22.22, a* = 22.45, b* = 5.09), reflecting excellent pigment preservation. Efficiency metrics revealed that − 20 °C achieved the highest nutrient retention per unit of energy consumed (g/MJ) for protein, carbohydrate, and fiber. In contrast, − 30 °C better preserved calcium and iron, while − 40 °C required the most energy yet yielded the lowest overall product quality. These findings identify − 20 °C as the optimal condition for VFD processing of Tiliacora triandra, supporting both scientific validity and practical application in functional food and herbal product development.