Analysis of heat input, microstructure evolution, crystallographic texture, and mechanical performance through layer-by-layer characterization of WAAM-fabricated Al–5Mg alloy
摘要
The present study involves analysis of the heat input, microstructure evolution, crystallographic texture and mechanical performance of Al–5Mg alloy deposited in a three-layer configuration. Samples were fabricated using single (SL), double (DL) and triple (TL) layer deposition at variable voltages (13–19.5 V), a gas flow rate of 10 l/min (99.99% Ar) and a wire feed rate of 4.1 m/min. Heat input was estimated using inverse heat conduction analysis. The estimated peak heat flux values for the third cycle of 14.5 V, 15 V and 19 V were 649 kW/m2, 505 kW/m2 and 1306 kW/m2 respectively. Heat flux transients were correlated with grain morphology. The average grain sizes and orientations at 14 V for SL, DL and TL deposition were 54.04 ± 2.36 µm 47.69 ± 2.60 µm and 59.28 ± 3.456 µm respectively with a [111] plane orientation. The average surface roughness of the 14.5 V sample was 3.89 µm and 14.64 µm for the second and third layers of deposition respectively. Fine equiaxed grains of average size 52 ± 3.2 µm with partially fused boundaries were observed for voltages in the range 15–16 V with the formation of β phase alongside the α-Al phase. The formation of β phase occurred near grain boundaries resulting in an increase in porosity by 10.35%. The grain size increased to 98 ± 8 µm for + 19 V deposition with an elongated columnar grain structure. For 19 V the average surface roughness was 47 µm across the three layers of deposition with higher porosity. Transmission electron microscopy revealed the formation of nanocrystalline precipitates and Mg2Al3 phase at a higher thermal gradient between the interlayers. Fractography revealed the formation of voids above 15 V while TEM analysis confirmed the presence of Mg2Al3 along the grain boundaries beyond 15 V suggesting that the formation of this intermetallic phase promoted void initiation at elevated voltages.