Near-Surface Microstructural Evolution and Hardening of Carburized M50NiL Steel under Repeated Laser Shock Peening
摘要
Repeated confined laser shock peening (LSP) was applied to carburized M50NiL steel to clarify the near-surface microstructural evolution and hardening behavior under repeated LSP. AFM, XRD, EBSD, nanoindentation, and residual-stress measurements were employed for characterization. Within approximately 150 μm from the treated surface, repeated LSP produced a clear gradient-affected layer, in which the effective martensitic block/sub-block size decreased from 1.38 μm (untreated) to 1.19 μm (LSP once) and 1.14 μm (LSP twice), while the corresponding low-angle grain boundary fraction increased from 25.1% to 31.4% and 35.2%. Surface/subsurface XRD showed a progressive decrease in retained austenite and an increase in dislocation density in both phases, with a stronger response in austenite than in martensite. EBSD-based recrystallization-state indicated that austenite evolved from a relatively recrystallized state toward a substructured state, whereas martensite mainly accommodated additional strain through defect rearrangement within the existing lath substructure. Repeated LSP also redistributed texture components and slightly increased the fraction of hard-oriented regions. Consequently, surface nanohardness increased from 8.62 GPa (untreated) to 11.62 GPa (LSP once) and 12.20 GPa (LSP twice), accompanied by a strong increase in compressive residual stress. The second pass provided only a reduced incremental hardening effect, indicating a partially saturated work-hardened state.