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<p>A simple-to-operate, environmentally friendly method has been developed for novel Ag sphere synthesis in NADES media to achieve spherical form and for green synthesis that was modified with MoS<sub>2</sub> nanoparticles. Ag@MoS<sub>2</sub> was designed as an adsorbent for a rapid and economical dispersive micro solid phase extraction approach at trace levels. The Analytical parameters pH (5.0), sorbent mass (10&#xa0;mg), extraction time (2.5&#xa0;min), eluent volume (5&#xa0;mL), eluent type (acetonitrile), and sample volume (10&#xa0;mL) were optimized. The detection limit was found to be 0.6&#xa0;μg L<sup>–1</sup> and the technique’s linearity ranged from 2.1 to 250&#xa0;μg L<sup>–1</sup>. The suggested approach has several benefits, including selectivity, precision, and rapidity. It is used practically to identify ATZ in lake water, fish farming water, tap water, allspice and rosehip. The ATZ recovery was sufficient, averaging between 91 and 107%. The method had an overall score of 0.57 on the AGREE scale.</p>

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Microwave Synthesis of Ag@MoS2 in NADES medium for the Dispersive Micro Solid Phase Extraction of Atrazine in environmental samples

  • 期刊论文

  • 出版模式：

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  • 发表日期：

    2025年4月16日

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  • Furkan Uzcan,
  • Mustafa Soylak

摘要

A simple-to-operate, environmentally friendly method has been developed for novel Ag sphere synthesis in NADES media to achieve spherical form and for green synthesis that was modified with MoS2 nanoparticles. Ag@MoS2 was designed as an adsorbent for a rapid and economical dispersive micro solid phase extraction approach at trace levels. The Analytical parameters pH (5.0), sorbent mass (10 mg), extraction time (2.5 min), eluent volume (5 mL), eluent type (acetonitrile), and sample volume (10 mL) were optimized. The detection limit was found to be 0.6 μg L–1 and the technique’s linearity ranged from 2.1 to 250 μg L–1. The suggested approach has several benefits, including selectivity, precision, and rapidity. It is used practically to identify ATZ in lake water, fish farming water, tap water, allspice and rosehip. The ATZ recovery was sufficient, averaging between 91 and 107%. The method had an overall score of 0.57 on the AGREE scale.