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<p>A&#xa0;new Tutton’s salt of Ammonium Zinc Nickel Sulphate Hexahydrate—AZNSH is proposed, which crystallizes in the monoclinic crystal system with the space group of P2<sub>1</sub>/c. The new crystal formula is (NH<sub>4</sub>)<sub>2</sub>Zn<sub><i>x</i></sub>Ni<sub>1–</sub><sub><i>x</i></sub>(SO<sub>4</sub>)<sub>2</sub>.6H<sub>2</sub>O with a&#xa0;formula weight of 397.45 at 296(2)&#xa0;K. The crystal formula ofH<sub>20</sub>N<sub>2</sub>Ni<sub>0.59</sub>O<sub>14</sub>S<sub>2</sub>Zn<sub>0.41</sub> gives the following lattice data: 6.2412(3), 12.4915(6), and 9.2080(5) Å for the <i>a, b</i> and <i>c</i>&#xa0;lattice parameters, whereas β = 106.941&#xa0;(2)° which is grown by slow evaporation solution growth method. The frequency enhancement by the AZNSH-coated diodes and the sensor efficiency of the specimens are reported. The new structure formulation is supported with the data on the lattice, electronic structure and with the crystal-sensor data.</p>

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Synthesis, structural analysis and studies of a novel Tutton’s salt—AZNSH crystal (NH4)2M(SO4)2.6H2O (M = Zn, Ni) grown by slow evaporation solution growth method for varied electronic and varied sensor applications

  • 期刊论文

  • 发表日期：

    2025年9月1日

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  • M. Sathish,
  • T. Balakrishnan,
  • P. Divya,
  • K. S. Radha,
  • Mohamed Abbas,
  • K. SenthilKannan

摘要

A new Tutton’s salt of Ammonium Zinc Nickel Sulphate Hexahydrate—AZNSH is proposed, which crystallizes in the monoclinic crystal system with the space group of P21/c. The new crystal formula is (NH4)2ZnxNi1–x(SO4)2.6H2O with a formula weight of 397.45 at 296(2) K. The crystal formula ofH20N2Ni0.59O14S2Zn0.41 gives the following lattice data: 6.2412(3), 12.4915(6), and 9.2080(5) Å for the a, b and c lattice parameters, whereas β = 106.941 (2)° which is grown by slow evaporation solution growth method. The frequency enhancement by the AZNSH-coated diodes and the sensor efficiency of the specimens are reported. The new structure formulation is supported with the data on the lattice, electronic structure and with the crystal-sensor data.