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<p>A convenient method for the C(sp<sup>3</sup>)H-functionalization of 2,9-dimethyl-1,10-phenanthroline (neocuproine) by the reaction with ethyl trifluoropyruvate was proposed. The reaction carried out by reflux in 1,2-dichloroethane gave 2,2′-(1,10-phenanthroline-2,9-diyl)bis(methylene)]bis(2-hydroxy-3,3,3-trifluoropropanoic acid) derivatives.</p>

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Novel route of neocuproine functionalization

  • 期刊论文

  • 发表日期：

    2025年1月1日

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  • E. S. Spesivaya,
  • Dzh. N. Konshina,
  • F. A. Kolokolov,
  • V. V. Konshin

摘要

A convenient method for the C(sp3)H-functionalization of 2,9-dimethyl-1,10-phenanthroline (neocuproine) by the reaction with ethyl trifluoropyruvate was proposed. The reaction carried out by reflux in 1,2-dichloroethane gave 2,2′-(1,10-phenanthroline-2,9-diyl)bis(methylene)]bis(2-hydroxy-3,3,3-trifluoropropanoic acid) derivatives.