<p>The present study reports the synthesis of a magnesium-based benzene-1,4-dicarboxylate (Mg-BDC) metal-organic framework (MOF) using a solvothermal method. The synthesized Mg-BDC MOF was characterized to investigate its morphological, structural, electronic, and optical properties. Structural analysis was carried out using X-ray diffraction (XRD), while surface morphology and particle features are&#xa0;examined by scanning electron microscopy (SEM). The elemental composition and distribution are investigated and confirmed through energy-dispersive X-ray spectroscopy (EDS). Furthermore, the bonding interactions and functional groups are obtained using Fourier-transform infrared spectroscopy (FTIR). Photoluminescence (PL) investigations are employed to explore the optical emission properties of the Mg-BDC. The obtained results provide insight into the crystallographic arrangement, morphology, elemental composition, metal-ligand coordination, and optical characteristics of the Mg-BDC MOF. These findings highlight the structural stability and functional features of the synthesized Mg-BDC MOF, indicating its potential relevance for future exploration in optoelectronic, sensing, and energy-related applications.</p>

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Synthesis and characterization of magnesium-BDC metal–organic framework via solvothermal method

  • Suryaji N. Mane,
  • Sadhu K. Kolekar,
  • Sanjay D. Dhole,
  • Kailash B. Sapnar

摘要

The present study reports the synthesis of a magnesium-based benzene-1,4-dicarboxylate (Mg-BDC) metal-organic framework (MOF) using a solvothermal method. The synthesized Mg-BDC MOF was characterized to investigate its morphological, structural, electronic, and optical properties. Structural analysis was carried out using X-ray diffraction (XRD), while surface morphology and particle features are examined by scanning electron microscopy (SEM). The elemental composition and distribution are investigated and confirmed through energy-dispersive X-ray spectroscopy (EDS). Furthermore, the bonding interactions and functional groups are obtained using Fourier-transform infrared spectroscopy (FTIR). Photoluminescence (PL) investigations are employed to explore the optical emission properties of the Mg-BDC. The obtained results provide insight into the crystallographic arrangement, morphology, elemental composition, metal-ligand coordination, and optical characteristics of the Mg-BDC MOF. These findings highlight the structural stability and functional features of the synthesized Mg-BDC MOF, indicating its potential relevance for future exploration in optoelectronic, sensing, and energy-related applications.