<p>Bulk pure Cu and Cu-5Fe (wt%) materials were successfully fabricated at room temperature by powder consolidation using high-pressure torsion (HPT) processing through 30 turns under a pressure of 6 GPa. The microstructure, texture and mechanical properties of the fabricated bulk discs were systematically characterized across their diameters using electron backscatter diffraction, scanning electron microscopy, transmission electron microscopy, X-ray diffraction and Vickers microhardness. Additionally, their thermal stability was evaluated after annealing treatment at 500&#xa0;°C for 6&#xa0;h. The results show that two grain refinement stages occurred in the Cu disc accompanied by the formation of partial <i>A</i>-fibre (<InlineEquation ID="IEq1"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="10853_2025_11534_Article_IEq1.gif" Format="GIF" Height="18" Rendition="HTML" Resolution="72" Type="Linedraw" Width="22" /> </InlineMediaObject> <EquationSource Format="TEX">\({A}_{1}^{*}\)</EquationSource> <EquationSource Format="MATHML"><math> <mmultiscripts> <mi>A</mi> <mrow> <mn>1</mn> </mrow> <mrow> <mrow /> <mo>∗</mo> </mrow> </mmultiscripts> </math></EquationSource> </InlineEquation>/<InlineEquation ID="IEq2"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="10853_2025_11534_Article_IEq2.gif" Format="GIF" Height="18" Rendition="HTML" Resolution="72" Type="Linedraw" Width="22" /> </InlineMediaObject> <EquationSource Format="TEX">\({A}_{2}^{*}\)</EquationSource> <EquationSource Format="MATHML"><math> <mmultiscripts> <mi>A</mi> <mrow> <mn>2</mn> </mrow> <mrow> <mrow /> <mo>∗</mo> </mrow> </mmultiscripts> </math></EquationSource> </InlineEquation> and <i>A</i> components). The dynamic recrystallization was delayed in the Cu-5Fe disc owing to the pinning effect of Fe content. Consequently, the grain refinement was more effective, and the texture gradually developed the <i>B</i>,<i> A</i> and <InlineEquation ID="IEq3"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="10853_2025_11534_Article_IEq1.gif" Format="GIF" Height="18" Rendition="HTML" Resolution="72" Type="Linedraw" Width="22" /> </InlineMediaObject> <EquationSource Format="TEX">\({A}_{1}^{*}\)</EquationSource> <EquationSource Format="MATHML"><math> <mmultiscripts> <mi>A</mi> <mrow> <mn>1</mn> </mrow> <mrow> <mrow /> <mo>∗</mo> </mrow> </mmultiscripts> </math></EquationSource> </InlineEquation> components. The Cu-5Fe disc was harder than the Cu disc, and the microhardness increased across the disc diameter. Rapid grain growth with a high amount of Cu<sub>2</sub>O oxide and retained texture were the main characteristics of the annealed Cu disc. The precipitation of Fe phase during annealing led to the development of a duplex microstructure at the centre and mid-radius positions and a stable microstructure at the edge of the Cu-5Fe disc. Eventually, the annealing texture was transformed into a complete <i>A</i>-fibre (<InlineEquation ID="IEq4"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="10853_2025_11534_Article_IEq1.gif" Format="GIF" Height="18" Rendition="HTML" Resolution="72" Type="Linedraw" Width="22" /> </InlineMediaObject> <EquationSource Format="TEX">\({A}_{1}^{*}\)</EquationSource> <EquationSource Format="MATHML"><math> <mmultiscripts> <mi>A</mi> <mrow> <mn>1</mn> </mrow> <mrow> <mrow /> <mo>∗</mo> </mrow> </mmultiscripts> </math></EquationSource> </InlineEquation>/<InlineEquation ID="IEq5"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="10853_2025_11534_Article_IEq2.gif" Format="GIF" Height="18" Rendition="HTML" Resolution="72" Type="Linedraw" Width="22" /> </InlineMediaObject> <EquationSource Format="TEX">\({A}_{2}^{*}\)</EquationSource> <EquationSource Format="MATHML"><math> <mmultiscripts> <mi>A</mi> <mrow> <mn>2</mn> </mrow> <mrow> <mrow /> <mo>∗</mo> </mrow> </mmultiscripts> </math></EquationSource> </InlineEquation> and <i>A/</i><InlineEquation ID="IEq6"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="10853_2025_11534_Article_IEq6.gif" Format="GIF" Height="17" Rendition="HTML" Resolution="72" Type="Linedraw" Width="17" /> </InlineMediaObject> <EquationSource Format="TEX">\(\overline{A }\)</EquationSource> <EquationSource Format="MATHML"><math> <mover> <mi>A</mi> <mo>¯</mo> </mover> </math></EquationSource> </InlineEquation> components) which was quite similar to the Cu disc. The microhardness decreased after annealing but it was more homogeneously distributed across the disc diameter than the HPT-processed disc. The results were discussed based on the different grain refinement mechanisms, static recrystallization mechanisms, solute elements, dislocations and annealing twins.</p>

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Characterization of Cu-5Fe (wt.%) fabricated by powder consolidation using high-pressure torsion

  • Amar Djemli,
  • Hiba Azzeddine,
  • Piotr Bazarnik,
  • Foudil Sahnoune,
  • Yi Huang,
  • Thierry Baudin,
  • François Brisset,
  • Megumi Kawasaki,
  • Terence G. Langdon

摘要

Bulk pure Cu and Cu-5Fe (wt%) materials were successfully fabricated at room temperature by powder consolidation using high-pressure torsion (HPT) processing through 30 turns under a pressure of 6 GPa. The microstructure, texture and mechanical properties of the fabricated bulk discs were systematically characterized across their diameters using electron backscatter diffraction, scanning electron microscopy, transmission electron microscopy, X-ray diffraction and Vickers microhardness. Additionally, their thermal stability was evaluated after annealing treatment at 500 °C for 6 h. The results show that two grain refinement stages occurred in the Cu disc accompanied by the formation of partial A-fibre ( \({A}_{1}^{*}\) A 1 / \({A}_{2}^{*}\) A 2 and A components). The dynamic recrystallization was delayed in the Cu-5Fe disc owing to the pinning effect of Fe content. Consequently, the grain refinement was more effective, and the texture gradually developed the B, A and \({A}_{1}^{*}\) A 1 components. The Cu-5Fe disc was harder than the Cu disc, and the microhardness increased across the disc diameter. Rapid grain growth with a high amount of Cu2O oxide and retained texture were the main characteristics of the annealed Cu disc. The precipitation of Fe phase during annealing led to the development of a duplex microstructure at the centre and mid-radius positions and a stable microstructure at the edge of the Cu-5Fe disc. Eventually, the annealing texture was transformed into a complete A-fibre ( \({A}_{1}^{*}\) A 1 / \({A}_{2}^{*}\) A 2 and A/ \(\overline{A }\) A ¯ components) which was quite similar to the Cu disc. The microhardness decreased after annealing but it was more homogeneously distributed across the disc diameter than the HPT-processed disc. The results were discussed based on the different grain refinement mechanisms, static recrystallization mechanisms, solute elements, dislocations and annealing twins.