<p>This study examines the synthesis of YAG:Ce precursor powder and luminescent ceramics by reverse chemical co-precipitation. We investigated the effects of sintering additives (CaO, MgO, and TEOS), Ce<sup>3+</sup> activator concentration, vacuum sintering temperature, and the temperature of air annealing on the luminescent properties of YAG:Ce ceramics. The optimal parameters for achieving high luminescence efficiency were defined: sintering additive concentration of 0.01 wt.%, TEOS as the sintering additive, vacuum sintering temperature of 1800°C, and air annealing temperature of 600°C for TEOS-containing samples. A ceramic sample exhibiting a luminescence efficiency of 319 lm/W was achieved under laser radiation with a power of 190 mW and a spot diameter of approximately 5 mm.</p>

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Preparation of YAG:Ce Ceramics with High Luminescent Properties

  • V. A. Lapin,
  • A. A. Kravtsov,
  • V. A. Tarala,
  • V. E. Suprunchuk,
  • F. F. Malyavin,
  • D. S. Vakalov

摘要

This study examines the synthesis of YAG:Ce precursor powder and luminescent ceramics by reverse chemical co-precipitation. We investigated the effects of sintering additives (CaO, MgO, and TEOS), Ce3+ activator concentration, vacuum sintering temperature, and the temperature of air annealing on the luminescent properties of YAG:Ce ceramics. The optimal parameters for achieving high luminescence efficiency were defined: sintering additive concentration of 0.01 wt.%, TEOS as the sintering additive, vacuum sintering temperature of 1800°C, and air annealing temperature of 600°C for TEOS-containing samples. A ceramic sample exhibiting a luminescence efficiency of 319 lm/W was achieved under laser radiation with a power of 190 mW and a spot diameter of approximately 5 mm.