<p>It is assumed that the existence of dinitrosyl iron complexes (DNIC) with thiol-containing ligands in paramagnetic cationic or anionic forms (with d<sup>7</sup> or d<sup>9</sup> electron configurations of iron, respectively, described in the Enemark-Feltman representation by the formulas <b>[Fe(NO)</b><sub><b>2</b></sub><b>]</b><sup><b>7</b></sup> and <b>[Fe(NO)</b><sub><b>2</b></sub><b>]</b><sup><b>9</b></sup><b>)</b> is determined by the mechanism of formation of these complexes. The cationic form arises as a result of the disproportionation reaction of two NO molecules bound to the Fe<sup>2+</sup> ion, whereas the anionic form of DNIC is formed as a result of one-electron reduction of the mononitrosyl Fe<sup>2+</sup> complex by one of the two thiol-containing ligands, followed by the addition of a second NO molecule to the complex. In the absence of solvent, both forms of DNIC are characterized by a tetrahedral spatial structure. When dissolved in water, the cationic form, incorporating two water molecules, acquires a four-coordinated square-planar structure, the upper molecular orbital of which is characterized by the inclusion of the d<sub>z</sub>2 orbital of iron. The mononuclear cationic form of DNIC with thiol-containing ligands and a predominant resonance structure <b>[(RS</b><sup><b>−</b></sup><b>)</b><sub><b>2</b></sub><b>Fe</b><sup><b>2+</b></sup><b>(NO)(NO</b><sup><b>+</b></sup><b>)]</b><sup><b>+</b></sup> is capable of acting in living organisms as donors of both NO molecules and nitrosonium cations.</p>

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Dinitrosyl Iron Complexes with Thiol-Containing Ligands in Aqueous Solution are Presented in their Cationic form with the d7 Electronic Configuration of Iron (Review)

  • A. F. Vanin

摘要

It is assumed that the existence of dinitrosyl iron complexes (DNIC) with thiol-containing ligands in paramagnetic cationic or anionic forms (with d7 or d9 electron configurations of iron, respectively, described in the Enemark-Feltman representation by the formulas [Fe(NO)2]7 and [Fe(NO)2]9) is determined by the mechanism of formation of these complexes. The cationic form arises as a result of the disproportionation reaction of two NO molecules bound to the Fe2+ ion, whereas the anionic form of DNIC is formed as a result of one-electron reduction of the mononitrosyl Fe2+ complex by one of the two thiol-containing ligands, followed by the addition of a second NO molecule to the complex. In the absence of solvent, both forms of DNIC are characterized by a tetrahedral spatial structure. When dissolved in water, the cationic form, incorporating two water molecules, acquires a four-coordinated square-planar structure, the upper molecular orbital of which is characterized by the inclusion of the dz2 orbital of iron. The mononuclear cationic form of DNIC with thiol-containing ligands and a predominant resonance structure [(RS)2Fe2+(NO)(NO+)]+ is capable of acting in living organisms as donors of both NO molecules and nitrosonium cations.