<p>Under the Hurd–Mori reaction conditions, semicarbazones of 4-acetylfurancarboxylates and 4-oxo-4,5,6,7-tetrahydrobenzofurancarboxylates are converted into 1,2,3-thiadiazolylfurancarboxylates or furo[1,2,3]benzothiadiazolecarboxylates. The structure of the synthesized heterocycles is characterized by a set of spectral methods and by X-ray diffraction analysis.</p> Graphical abstract <p></p>

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Synthesis of new 1,2,3-thiadiazole-containing furancarboxylates

  • Kirill A. Gomonov,
  • Vasilii V. Pelipko,
  • Igor A. Litvinov,
  • Ruslan I. Baichurin,
  • Sergey V. Makarenko

摘要

Under the Hurd–Mori reaction conditions, semicarbazones of 4-acetylfurancarboxylates and 4-oxo-4,5,6,7-tetrahydrobenzofurancarboxylates are converted into 1,2,3-thiadiazolylfurancarboxylates or furo[1,2,3]benzothiadiazolecarboxylates. The structure of the synthesized heterocycles is characterized by a set of spectral methods and by X-ray diffraction analysis.

Graphical abstract