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<p>The TiNi and ZnO powders were mixed at a 1:1 ratio and mechanically milled for 30 and 60&#xa0;h, respectively. The XRD analysis of the milled powder revealed a predominantly single broad peak after 30 and 60&#xa0;h. Raman analysis also revealed a broad peak indicative of the short-range order or lack of crystallinity due to MM. TEM images showed the lattice fringes with a decreased number of diffraction rings due to the partial formation of amorphous particles complementing the XRD and Raman results. Thermal analysis showed an exothermic peak at 543&#xa0;°C, while no exothermic peak has emerged in the 60&#xa0;h milled ZnO-TiNi powder.</p>

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Alloying ZnO with TiNi powders through mechanical milling followed by annealing

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  • 发表日期：

    2025年9月4日

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  • Amogelang S. Bolokang

摘要

The TiNi and ZnO powders were mixed at a 1:1 ratio and mechanically milled for 30 and 60 h, respectively. The XRD analysis of the milled powder revealed a predominantly single broad peak after 30 and 60 h. Raman analysis also revealed a broad peak indicative of the short-range order or lack of crystallinity due to MM. TEM images showed the lattice fringes with a decreased number of diffraction rings due to the partial formation of amorphous particles complementing the XRD and Raman results. Thermal analysis showed an exothermic peak at 543 °C, while no exothermic peak has emerged in the 60 h milled ZnO-TiNi powder.